منابع مشابه
Gas-liquid chromatographic determination
A method for the determination of total bile acids in human feces that is suitable for routine application is described and discussed. Bile acids are extracted from freezedried feces with acetic acid and toluene, in the presence of the i?ternal standard 23-nordeoxycholic acid. After saponification of the extract, bile acids and the internal standard are methylated and converted by mild chromic ...
متن کاملHIGH-PERFORMANCE LIQUID CHROMATOGRAPHIC DETERMINATION OF THEOPHYLLINE IN HUMAN SERUM
A simple, rapid and sensitive HPLC method for the determination of theophylline (T) in human serum has been developed. An isocratic system consisting of a /-l Bondapak C18 column, mobile phase of methanol, phosphate buffer (22:78, pH=4.5), and a flow rate of 1.4 mL/min was used. The eluent was detected by UV at 275 nm at room temperature. 8-Chlorotheophylline (8-CT) was used as an internal ...
متن کاملLiquid-chromatographic determination of nadolol in plasma.
We describe a liquid-chromatographic procedure for determining nadolol in plasma. After an analog of nadolol is added as internal standard, the plasma sample is passed through a disposable BondElut C18 column. After several column washes, nadolol and the internal standard are eluted with methanol, and the eluate is evaporated and reconstituted with the mobile phase (acetonitrile/water, perchlor...
متن کاملLiquid Chromatographic Determination of Ornithine and Lysine
with Krebs–Henseleit cycle and polyamine synthesis.1–3 It was reported that their high concentration levels in plasma and urine were indicative in diagnoses of some congenital metabolic disorders like cystinuria or hyperlysinemia.2–4 Thus, the selective determination of ornithine and lysine might be more valuable for the diagnoses of these disorders. An amino acids analyzer based on derivatizat...
متن کاملLiquid-chromatographic determination of aminoglutethimide in plasma.
A simple, rapid "high-performance" liquid-chromatographic procedure is presented for the determination of aminoglutethimide in plasma. After precipitation of the protein with acetonitrile, an aliquot of the supernate is injected directly onto a radially compressed, reversed-phase column. The aminoglutethimide is isocratically eluted with a mobile phase of acetonitrile/water/tert-butyl ammonium ...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Journal of AOAC INTERNATIONAL
سال: 1964
ISSN: 0095-9111
DOI: 10.1093/jaoac/47.2.264